HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 54209658, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Chloroacetone | HCID 6571 | — |
| Reactant | O-tert-butylhydroxylamine hydrochloride | HCID 2777906 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 54209658 | HCID 54209658 | — |
Reaction Steps
A mixture of 1.51 g of O-tert-butylhydroxylamine hydrochloride, 0.93 g of chloroacetone, and 10 ml of diethyl ether is stirred at room temperature for 3 hours, poured into water, and extracted twice with diethyl ether. The diethyl ether layers are combined, washed with water, dried over anhydrous magnesium sulfate, and concentrated, which affords chloroacetone O-tert-butyloxime.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06437184B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-3b810c26081e4461a78439f116078579 |
| Source note | uspto-grants-2002_08 |