Hydrochloric Acid → HCID 21954458, compound

Participants

Reaction Steps

A mixture of 10 mmole of the above-prepared 1-(1-methacryloyloxy-1-methylethyl)-3,5-bis(2-methoxyethoxymethoxy)adamantane, 1 mmole (in terms of HCl) of 6 N-HCl, and 40 ml of acetone was stirred at room temperature for 5 hours. An aqueous ammonium chloride solution was added to the reaction mixture; the resulting mixture was extracted with ethyl acetate; the organic layer was concentrated; and the concentrate was subjected to column chromatography on a silica gel to yield the title compound.

Provenance & Evidence