Acryloyl chloride → 3,5-Dihydroxy-1-adamantyl methacrylate

HRID 2305280Notes

Reaction equation

HRID 2305280 reaction equation
[C:1]12([OH:13])[CH2:10][C:5]3([OH:11])[CH2:6][CH:7]([CH2:9][C:3]([OH:12])([CH2:4]3)[CH2:2]1)[CH2:8]2.[C:14](Cl)(=[O:18])[C:15]([CH3:17])=[CH2:16].C12(O)CC3CC(CC(O)(C3)C1)C2.C(Cl)(=O)C=C>>[OH:13][C:1]12[CH2:10][C:5]3([O:11][C:14](=[O:18])[C:15]([CH3:17])=[CH2:16])[CH2:6][CH:7]([CH2:9][C:3]([OH:12])([CH2:4]3)[CH2:2]1)[CH2:8]2

Participants

5

Reactant 4

HCID 13140Acryloyl chlorideHCID 13528Methacryloyl chlorideHCID 5738291,3-AdamantanediolHCID 98990221,3,5-Adamantanetriol

Product 1

HCID 130073943,5-Dihydroxy-1-adamantyl methacrylate

Procedure

The title compound was prepared in the same manner as in Production Example 6, except that 1,3,5-adamantanetriol and methacrylic chloride were used instead of 1,3-adamantanediol and acrylic chloride, respectively.

Sources & evidence

ORD record
ord-3333ea1e07474971bc63cb7683b11d73
Source dataset
uspto-grants-2002_08
Patent number
US06440636B1

Reaction notes

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