HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl isothiocyanate → HCID 18432474, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl isothiocyanate | HCID 11167 | — |
| Reactant | (2,2-Diethoxyethyl)hydrazine | HCID 322952 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18432474 | HCID 18432474 | — |
Reaction Steps
A mixture of 4 g of hydrazino-acetaldehyd diethylacetal in 40 ml of ethanol is stirred with 1.97 g of methylisothiocyanate for ca. 4 hours at room temperature, the solvent is evaporated off and 2-(2,2-diethoxy-ethyl)-4-methyl-thiosemicarbazide is obtained in crystalline form.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06440957B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-c62f038de00349c4aaf47efbf2e3e097 |
| Source note | uspto-grants-2002_08 |