HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 178486089, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178486089 | HCID 178486089 | — |
Reaction Steps
To a stirring solution comprised of para-toluenesulfonyl chloride in dichloromethane at 0° C. is introduced excess gaseous dimethylamine. The precipitate is removed by filtration and the filtrate is concentrated in vacuo to obtain the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06440966B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-28fa3bcc403348eb8fab9aa23079806e |
| Source note | uspto-grants-2002_08 |