Dimethylamine → HCID 178486089, compound

HRID 2305331Notes

Reaction equation

HRID 2305331 reaction equation
[C:1]1([CH3:11])[CH:6]=[CH:5][C:4]([S:7](Cl)(=[O:9])=[O:8])=[CH:3][CH:2]=1.[CH3:12][NH:13][CH3:14]>ClCCl>[CH3:11][C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:12][N:13]([CH3:14])[SH:7](=[O:9])=[O:8]

Participants

4

Reactant 2

HCID 674DimethylamineHCID 73974-Toluenesulfonyl chloride

Product 1

HCID 178486089HCID 178486089, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

To a stirring solution comprised of para-toluenesulfonyl chloride in dichloromethane at 0° C. is introduced excess gaseous dimethylamine. The precipitate is removed by filtration and the filtrate is concentrated in vacuo to obtain the product.

Workup

  1. customThe precipitate is removed by filtration
  2. concentrationthe filtrate is concentrated in vacuo
  3. customto obtain the product

Sources & evidence

ORD record
ord-28fa3bcc403348eb8fab9aa23079806e
Source dataset
uspto-grants-2002_08
Patent number
US06440966B1

Reaction notes

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