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HRID23054

反应详情

EQUATION

反应方程式

HRID 23054 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)C(C)=O
HCID11748

Methylpyruvate

C4H6O3

结构：COC(=O)[C@H](C)Nc1ccc2c(c1)OCCO2
HCID53867794

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)COC(=O)[C@H](C)Nc1ccc2c(c1)OCCO2
HCID53856555

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)CO
溶剂HCID6560

2-Methyl-1-propanol

C4H10O

PROCEDURE

实验过程

Following reductive amination General Procedure AA above and using 1,4-benzodioxa-6-amine (Aldrich) and methyl pyruvate (Aldrich), N-(3,4-ethylenedioxyphenyl)alanine methyl ester was prepared. The methyl ester was then transesterified following General Procedure AQ above using iso-butanol to provide the title compound. Purification was by preparative plate chromatography.

WORKUP

后处理

  1. customwas prepared