Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl pyruvate → N-(3,4-ethylenedioxyphenyl)alanine Iso-butyl Ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl pyruvate | HCID 11748 | — |
| 반응물 | N-(3,4-ethylenedioxyphenyl)alanine methyl ester | HCID 53867794 | — |
| 용매 | Isobutanol | HCID 6560 | — |
| 생성물 | N-(3,4-ethylenedioxyphenyl)alanine Iso-butyl Ester | HCID 53856555 | — |
반응 단계
Following reductive amination General Procedure AA above and using 1,4-benzodioxa-6-amine (Aldrich) and methyl pyruvate (Aldrich), N-(3,4-ethylenedioxyphenyl)alanine methyl ester was prepared. The methyl ester was then transesterified following General Procedure AQ above using iso-butanol to provide the title compound. Purification was by preparative plate chromatography.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06849650B2 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-7c12d267fe1f41bd994b7c07dd3a6b03 |
| 출처 메모 | uspto-grants-2005_02 |