HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methane → HCID 178454477, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methane | HCID 297 | — |
| Reactant | Butyryl chloride | HCID 8855 | — |
| Reactant | HCID 178508000 | HCID 178508000 | — |
| Product | HCID 178454477 | HCID 178454477 | 46.3% |
Reaction Steps
Using the general method of Example 57 Part B, 3-amino[1,5]naphthyridin-4-ol (1.8 g, 11.2 mmol) was reacted with butyryl chloride (1.3 g, 12.3 mmol) to provide 1.2 g of N-(4-hydroxy[1,5]naphthyridin-3-yl)butanamide as a charcoal gray solid, m.p.>360° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06440992B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-011a127d60ac49a8b1eefd93dcf24684 |
| Source note | uspto-grants-2002_08 |