Butyl iodide → HCID 86587903, compound

HRID 2305797Notes

Reaction equation

HRID 2305797 reaction equation
[OH:1][C:2]1[CH:9]=[CH:8][CH:7]=[CH:6][C:3]=1[C:4]#N.I[CH2:11][CH2:12][CH2:13][CH3:14].[C:15]([NH:19][OH:20])([CH3:18])([CH3:17])[CH3:16]>>[CH2:11]([O:1][C:2]1[CH:9]=[CH:8][CH:7]=[CH:6][C:3]=1[CH:4]=[N+:19]([C:15]([CH3:18])([CH3:17])[CH3:16])[O-:20])[CH2:12][CH2:13][CH3:14]

Participants

4

Reactant 3

HCID 10962Butyl iodideHCID 119072-HydroxybenzonitrileHCID 98586N-tert-butylhydroxylamine

Product 1

HCID 86587903HCID 86587903, compound

Procedure

The title compound was prepared according to the procedure described in Example 28 using 2-hydroxybenzonitrile, 1-iodobutane and N-tert-butylhydroxylamine. The title compound was isolated in 77.4% overall yield as a viscous oil.

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-4726e3bbc8dd4303b32a4840c91bdada
Source dataset
uspto-grants-2002_08
Patent number
US06441032B1

Reaction notes

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