HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexylhydroxylamine → alpha-(4-Benzyloxyphenyl)-N-cyclohexylnitrone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexylhydroxylamine | HCID 72935 | — |
| Reactant | Benzaldehyde, 4-(phenylmethoxy)- | HCID 78109 | — |
| Product | alpha-(4-Benzyloxyphenyl)-N-cyclohexylnitrone | HCID 86587911 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 42 using 4-benzyloxybenzaldehyde and N-cyclohexylhydroxylamine. The title compound was obtained in 81.2% yield as slightly yellowish solid, m.p. 129.0° C. (Rf=0.30 on a silica gel plate using hexanes:EtOAc, 1:1, v:v, as an eluant).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06441032B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-ff102cbda256458f852acf2713a9c579 |
| Source note | uspto-grants-2002_08 |