HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxybenzaldehyde → alpha-(2-methoxyphenyl)-N-t-butylnitrone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxybenzaldehyde | HCID 8658 | — |
| Reactant | N-tert-butylhydroxylamine | HCID 98586 | — |
| Product | alpha-(2-methoxyphenyl)-N-t-butylnitrone | HCID 85447185 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 7 using 2-methoxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 82.9% overall yield as white crystals, m.p. 109.1° C. (Rf=0.53 on a silica gel plate using ethyl acetate as the eluant).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06441032B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-278ef9eefb9741c5bf9582b4aedf707c |
| Source note | uspto-grants-2002_08 |