HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 18433615, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 18433594 | HCID 18433594 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 18433615 | HCID 18433615 | — |
Reaction Steps
A solution of 1-(tert-butoxycarbonylamino)-7-(tert-butyldimethylsilyloxy)naphthalene, as described above in Step B, (5.00 g, 13.4 mmol) in EtOAc (240 mL) and Et2O (60 mL) at ambient temperature was saturated with HCl (g). After 1 hour, the mixture was concentrated in vacuo to yield the desired product as a pale solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06441017B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-b9125213566a4c12a1d49dde9af3ebce |
| Source note | uspto-grants-2002_08 |