Water → HCID 18433491, compound

Participants

Reaction Steps

3-Aminoquinoline (6.04 g, 41.89 mmol) and Et3N (5.85 mL, 41.89 mmol) were dissolved in CH2Cl2 (75 mL). Acetic anhydride (3.95 mL, 41.89 mmol) was added and reaction stirred at ambient temperature for 18 hours. The reaction mixture was poured into H2O and filtered. The filtered solid was dried in vacuo to yield the above-titled compound.

Provenance & Evidence