HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl iodide → HCID 17902130, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl iodide | HCID 10962 | — |
| Reactant | 3H-Indole, 2,3,3-trimethyl-5-nitro- | HCID 97551 | — |
| Product | HCID 17902130 | HCID 17902130 | — |
Reaction Steps
5-Nitro-2,3,3-trimethylindole (250 mg, 1.22 mmol) and iodobutane (10 ml, 16.17 g, 87.87 mmol) were mixed and heated to reflux for 16hrs. The solvent was removed and the impure material stored at−20° C. for use in later reactions.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06828116B1 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-0bfeec58765445f6a35d1b465bfbc39c |
| Source note | uspto-grants-2004_12 |