Butyl iodide → HCID 17902130, compound

HRID 2306534Notes

Reaction equation

HRID 2306534 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]2[C:10](=[CH:11][CH:12]=1)[N:9]=[C:8]([CH3:13])[C:7]2([CH3:15])[CH3:14])([O-:3])=[O:2].[I:16][CH2:17][CH2:18][CH2:19][CH3:20]>>[I-:16].[CH2:17]([N+:9]1[C:10]2[C:6](=[CH:5][C:4]([N+:1]([O-:3])=[O:2])=[CH:12][CH:11]=2)[C:7]([CH3:15])([CH3:14])[C:8]=1[CH3:13])[CH2:18][CH2:19][CH3:20]

Participants

3

Reactant 2

HCID 10962Butyl iodideHCID 975513H-Indole, 2,3,3-trimethyl-5-nitro-

Product 1

HCID 17902130HCID 17902130, compound

Procedure

5-Nitro-2,3,3-trimethylindole (250 mg, 1.22 mmol) and iodobutane (10 ml, 16.17 g, 87.87 mmol) were mixed and heated to reflux for 16hrs. The solvent was removed and the impure material stored at−20° C. for use in later reactions.

Workup

  1. temperatureheated
  2. temperatureto reflux for 16hrs
  3. customThe solvent was removed
  4. custom20° C.

Sources & evidence

ORD record
ord-0bfeec58765445f6a35d1b465bfbc39c
Source dataset
uspto-grants-2004_12
Patent number
US06828116B1

Reaction notes

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