HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 73985894, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | O-Methylhydroxylamine hydrochloride | HCID 521874 | — |
| Reactant | HCID 54183450 | HCID 54183450 | — |
| Product | HCID 73985894 | HCID 73985894 | — |
Reaction Steps
Methoxylamine hydrochloride (0.996 g, 0.0119 mol) is added to a solution of formylcinnamic acid (2 g, 0.0114 mol) in pyridine (20 ml) and is stirred for 2 hours. The reaction mixture is evaporated under vacuum and the residue is diluted with 2N aqueous HCl. The resulting precipitate is filtered and dried under vacuum (2.00 g, 85%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06828317B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-90bfc2b87ca44e94b3720a8f4a4f0c65 |
| Source note | uspto-grants-2004_12 |