HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10288183, compound → HCID 23529017, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10288183 | HCID 10288183 | — |
| Reactant | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Product | HCID 23529017 | HCID 23529017 | — |
Reaction Steps
20% Trifluoroacetic acid/dichloromethane (2 ml) is added to {3-[3-fluoro-4-(5-thioxo-5,6-dihydro-4H-[1,3,4]thiadiazin-2-yl)-phenyl]-2-oxo-oxazolidin-5(S)-ylmethyl}-carbamic acid tert-butyl ester and the mixture is stirred at room temperature for 30 minutes. The reaction is evaporated to dryness and the trifluoroacetate salt is used directly in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06828317B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-31dcb6254e9b422396e405bb841358bf |
| Source note | uspto-grants-2004_12 |