Hydrochloric Acid → HCID 22556503, compound

HRID 2306797Notes

Reaction equation

HRID 2306797 reaction equation
C([O:3][C:4]([C:6]1[NH:10][C:9]2[S:11][C:12]([Cl:14])=[CH:13][C:8]=2[C:7]=1[Cl:15])=[O:5])C.Cl>>[Cl:14][C:12]1[S:11][C:9]2[NH:10][C:6]([C:4]([OH:5])=[O:3])=[C:7]([Cl:15])[C:8]=2[CH:13]=1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 67550799HCID 67550799, compound

Product 1

HCID 22556503HCID 22556503, compound

Procedure

2,4-Dichloro-6H-thieno[2,3-b]pyrrole-5-carboxylic acid ethyl ester was hydrolyzed according to Procedure E (reflux for 12 h before allowing to cool to room temperature; acidification with concentrated HCl; no purification).

Workup

  1. temperaturereflux for 12 h
  2. customno purification)

Sources & evidence

ORD record
ord-072fb9d5b6d64cbbb24168c55a14cd85
Source dataset
uspto-grants-2004_12
Patent number
US06828343B2

Reaction notes

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