3-Azido-1,5,5-trimethyl-1-cyclohexene → HCID 22630126, compound

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Reaction Steps

Prepared from azide 34 according to the procedure for compound 11 (Example 3, c). Amine hydrochloride 35 obtained as a colorless solid in 57% yield. 1H NMR (CDCl3, TMS): 0.89 and 1.03 (total 6H, both s, 5,5-CH3); 1.25-2.15 (4H, m, 4,6-CH2); 1.72 (3H, s, 3-CH3); 3.88 (1H, m, 1-CH); 5.41 (1H, s, C═CH) and 8.40 ppm (3H, br s, NH3+).

Provenance & Evidence