Azide → HCID 22630141, compound

Participants

Reaction Steps

Prepared from azide 39 according to the procedure for compound 11 (Example 3, c). Amine hydrochloride 40 obtained as a colorless solid with 60% yield. 1H NMR (CDCl3, TMS): 0.96 and 1.07 (total 6H, both s, 5,5-CH3); 1.56 (3H, s, 1-CH3); 1.73 (3H, s, 3-CH3); 1.60-2.05 (4H, m, 4,6-CH2); 5.49 (1H, s, C═CH) and 8.27 ppm (3H, br s, NH3+).

Provenance & Evidence