Hydrochloric Acid → HCID 22605938, compound

Participants

Reaction Steps

Following the general method described in example 9, N-[2-(3,4-dihydro-1H-isoquinolin-2-yl)-pyridin-4-yl]-benzamide (example 17a) was reacted with lithium aluminum hydride. After workup and chromatography the free base of the title compound was treated with hydrogen chloride and triturated with Et2O/pentane. The title compound was obtained as white amorphous material. MS: m/e=315 (M+).

Provenance & Evidence