HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 6-(1-methyl-1H-pyrazol-4-yl)pyridine-3-carbonyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 3953327 | HCID 3953327 | — |
| Product | 6-(1-methyl-1H-pyrazol-4-yl)pyridine-3-carbonyl chloride | HCID 22605453 | — |
Reaction Steps
A suspension of 6-(1-methyl-1H-pyrazol-4-yl)pyridine-3-carboxylic acid (0.48 g) in thionyl chloride (5.0 ml) was stirred at room temperature for 2 hours. The volatile material was removed under reduced pressure to afford 6-(1-methyl-1H-pyrazol-4-yl)pyridine-3-carbonyl chloride as a solid, which was utilized without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06831079B1 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-f45e4fe917de4560b1c572e5040d1891 |
| Source note | uspto-grants-2004_12 |