HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 69919591, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 69850326 | HCID 69850326 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 69919591 | HCID 69919591 | — |
Reaction Steps
To a solution of 3-phenyl-N-[1-(1,2,3,4-tetrahydro-quinolin-7-yl)-ethyl]-acrylamide (Example 233) in CH2Cl2 at 0° C. was added triethylamine followed by acetyl chloride. Work up and flash chromatography provided the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06831080B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-2aa046afc70d4dd88d46cbf5181f84d0 |
| Source note | uspto-grants-2004_12 |