HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl chloroformate → HCID 69945511, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | HCID 69435312 | HCID 69435312 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 69945511 | HCID 69945511 | 73.3% |
Reaction Steps
A mixture of cis and trans 2-benzoyloxymethyl-5-hydroxy-1,3-oxathiolane 1.49 g (6.6 mmol) (as prepared in Example 1) was reacted with ethylchloroformate 1.3 mL (13.2 mmol) and pyridine (3.3 mL) as described in example 2 to give 1.51 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06831174B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-efa51da0856c4aeba2f0508082ba8889 |
| Source note | uspto-grants-2004_12 |