HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-iodobenzoate → 3'-Hydroxy-biphenyl-3-carboxylic acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-iodobenzoate | HCID 143542 | — |
| Reactant | (3-(Methoxymethoxy)phenyl)boronic acid | HCID 22606941 | — |
| Product | 3'-Hydroxy-biphenyl-3-carboxylic acid ethyl ester | HCID 22606886 | — |
Reaction Steps
In a manner similar to that of Example 1(h), by reaction of 2 g (13.3 mmol) of 3-methoxymethoxyphenylboronic acid with 1.83 mL (11 mmol) of ethyl 3-iodobenzoate, 1.9 g (72%) of the expected ethyl ester are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06831106B1 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-4e20bf254a6f4736904b5d3490b409fd |
| Source note | uspto-grants-2004_12 |