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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2307558Generated: November 4, 2026

Potassium Carbonate → Methyl 3'-[3,4-bis(1-phenylmethanoyloxymethyl)benzyloxy]-2'-methylbiphenyl-4-carboxylate

https://huagongshe.com/reaction/2307558

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant3,4-Bis(benzoyloxymethyl)benzyl bromideHCID 22345618—
ReactantMethyl 3'-hydroxy-2'-methylbiphenyl-4-carboxylateHCID 22606879—
ProductMethyl 3'-[3,4-bis(1-phenylmethanoyloxymethyl)benzyloxy]-2'-methylbiphenyl-4-carboxylateHCID 22606934—

Reaction Steps

In a manner similar to that of Example 1(i), by reaction of 1 g (4.1 mmol) of methyl 3′-hydroxy-2′-methylbiphenyl-4-carboxylate with 2 g (4.5 mmol) of 3,4-bis(benzoyloxymethyl)benzyl bromide and 650 mg (4.7 mmol) of potassium carbonate, the desired product is obtained in the form of a colourless oil (m=2.4 9; Y=97%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06831106B1
Source datasetuspto-grants-2004_12
ORD IDord-a9b9a78a925c4cc8a95341a865cd05f0
Source noteuspto-grants-2004_12