HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → Methyl 3'-[3,4-bis(1-phenylmethanoyloxymethyl)benzyloxy]-2'-methylbiphenyl-4-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3,4-Bis(benzoyloxymethyl)benzyl bromide | HCID 22345618 | — |
| Reactant | Methyl 3'-hydroxy-2'-methylbiphenyl-4-carboxylate | HCID 22606879 | — |
| Product | Methyl 3'-[3,4-bis(1-phenylmethanoyloxymethyl)benzyloxy]-2'-methylbiphenyl-4-carboxylate | HCID 22606934 | — |
Reaction Steps
In a manner similar to that of Example 1(i), by reaction of 1 g (4.1 mmol) of methyl 3′-hydroxy-2′-methylbiphenyl-4-carboxylate with 2 g (4.5 mmol) of 3,4-bis(benzoyloxymethyl)benzyl bromide and 650 mg (4.7 mmol) of potassium carbonate, the desired product is obtained in the form of a colourless oil (m=2.4 9; Y=97%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06831106B1 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-a9b9a78a925c4cc8a95341a865cd05f0 |
| Source note | uspto-grants-2004_12 |