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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2307568Generated: November 1, 2026

Potassium Carbonate → Ethyl 5'-[3,4-bis(1-phenylmethanoyloxymethyl)-benzyloxy]-2'-methylbiphenyl-4-carboxylate

https://huagongshe.com/reaction/2307568

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant3,4-Bis(benzoyloxymethyl)benzyl bromideHCID 22345618—
ReactantEthyl 5'-hydroxy-2'-methylbiphenyl-4-carboxylateHCID 22606906—
ProductEthyl 5'-[3,4-bis(1-phenylmethanoyloxymethyl)-benzyloxy]-2'-methylbiphenyl-4-carboxylateHCID 22606888—

Reaction Steps

In a manner similar to that of Example 1(i), by reaction of 3.07 g (12 mmol) of ethyl 5′-hydroxy-2′-methylbiphenyl-4-carboxylate with 6.7 g (15 mmol) of 3,4-bis(benzoyloxymethyl)benzyl bromide and 2 mg (14 mmol) of potassium carbonate, the desired product is obtained in the form of a colourless oil (m=5.7 g; Y=77%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06831106B1
Source datasetuspto-grants-2004_12
ORD IDord-877b03b68bf74828bc829fba7aed0cf9
Source noteuspto-grants-2004_12