HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 17934664, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 22606926 | HCID 22606926 | — |
| Product | HCID 17934664 | HCID 17934664 | — |
Reaction Steps
In a manner similar to that of Example 20(e), by reaction of 4.5 g (15.2 mmol) of 4′-(2-ethyl-[1,3]dioxolan-2-yl]-2′-methylbiphenyl-3-carbaldehyde with 760 mg (20 mmol) of lithium aluminium hydride, the desired product is obtained in the form of a colourless oil (m=4.4 g, Y=97%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06831106B1 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-f64981d19a734eea934650552bc6f6e8 |
| Source note | uspto-grants-2004_12 |