Aluminium lithium hydride → HCID 22606878, compound

Participants

Reaction Steps

In a manner similar to that of Example 20(e), by reaction of 1.5 g (3.15 mmol) of dimethyl 4-[4′(1-ethyl-1-hydroxypropyl)-2′-methylbiphenyl-3-ylmethoxy)-phthalate with 480 mg (12.6 mmol) of lithium aluminium hydride, the desired product is obtained in the form of a white solid (m.p.=87° C.; m=1.03 g; Y=78%).

Provenance & Evidence