Aluminium lithium hydride → HCID 69825607, compound

Participants

Reaction Steps

In a manner similar to that of Example 20(e), by reaction of 900 mg (2 mmol) of dimethyl 4-(2′-methyl-4′-propionylbiphenyl-3-ylmethoxy)phthalate (described in Example 22(f)) with 300 mg (8 mmol) of lithium aluminium hydride, the desired product is obtained in the form of a white solid (m.p.=78° C.; m=737 mg; Y=94%).

Provenance & Evidence