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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2307582Generated: October 31, 2026

Potassium Carbonate → Methyl 3'-[3,4-bis-(1-phenylmethanoyloxymethyl)benzyloxy]-3-methylbiphenyl-4-carboxylate

https://huagongshe.com/reaction/2307582

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant3,4-Bis(benzoyloxymethyl)benzyl bromideHCID 22345618—
ReactantMethyl 3'-hydroxy-3-methylbiphenyl-4-carboxylateHCID 22606892—
ProductMethyl 3'-[3,4-bis-(1-phenylmethanoyloxymethyl)benzyloxy]-3-methylbiphenyl-4-carboxylateHCID 22606954—

Reaction Steps

In a manner similar to that of Example 1(i), by reaction of 1.5 g (6.2 mmol) of methyl 3′-hydroxy-3-methylbiphenyl-4-carboxylate with 3 g (6.88 mmol) of 3,4-bis(benzoyloxymethyl)benzyl bromide and 900 mg (6.4 mmol) of potassium carbonate, the desired product is obtained in the form of a yellow oil (m=3.69 g; Y=99%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06831106B1
Source datasetuspto-grants-2004_12
ORD IDord-5cd81acb0b4442bda9a5afd6201d22b2
Source noteuspto-grants-2004_12