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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2307585Generated: October 31, 2026

Potassium Carbonate → Methyl 4'-[3,4-bis-(1-phenylmethanoyloxymethyl)-benzyloxy]-2-methylbiphenyl-4-carboxylate

https://huagongshe.com/reaction/2307585

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant3,4-Bis(benzoyloxymethyl)benzyl bromideHCID 22345618—
ReactantMethyl 4'-hydroxy-2-methylbiphenyl-4-carboxylateHCID 22606882—
ProductMethyl 4'-[3,4-bis-(1-phenylmethanoyloxymethyl)-benzyloxy]-2-methylbiphenyl-4-carboxylateHCID 22606924—

Reaction Steps

In a manner similar to that of Example 1(i), by reaction of 2.0 g (8.7 mmol) of methyl 4′-hydroxy-2-methylbiphenyl-4-carboxylate with 4.3 g (9.8 mmol) of 3,4-bis(benzoyloxymethyl)benzyl bromide and 1.29 g (9.3 mmol) of potassium carbonate, the desired product is obtained in the form of a yellow oil (m=4.88 g; Y=91%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06831106B1
Source datasetuspto-grants-2004_12
ORD IDord-ab2ac7296859449eaeee6a9b07d72f83
Source noteuspto-grants-2004_12