HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → Methyl 4'-[3,4-bis-(1-phenylmethanoyloxymethyl)-benzyloxy]-2-methylbiphenyl-4-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3,4-Bis(benzoyloxymethyl)benzyl bromide | HCID 22345618 | — |
| Reactant | Methyl 4'-hydroxy-2-methylbiphenyl-4-carboxylate | HCID 22606882 | — |
| Product | Methyl 4'-[3,4-bis-(1-phenylmethanoyloxymethyl)-benzyloxy]-2-methylbiphenyl-4-carboxylate | HCID 22606924 | — |
Reaction Steps
In a manner similar to that of Example 1(i), by reaction of 2.0 g (8.7 mmol) of methyl 4′-hydroxy-2-methylbiphenyl-4-carboxylate with 4.3 g (9.8 mmol) of 3,4-bis(benzoyloxymethyl)benzyl bromide and 1.29 g (9.3 mmol) of potassium carbonate, the desired product is obtained in the form of a yellow oil (m=4.88 g; Y=91%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06831106B1 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-ab2ac7296859449eaeee6a9b07d72f83 |
| Source note | uspto-grants-2004_12 |