HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → Methyl 4-bromo-2-methylbenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 4-Bromo-2-methylbenzoic acid | HCID 99570 | — |
| Catalyst | Hydrochloric Acid | HCID 313 | — |
| Product | Methyl 4-bromo-2-methylbenzoate | HCID 22031226 | 100% |
Reaction Steps
A solution of 4-bromo-2-methyl benzoic acid (1.0 g, 4.7 mmol) in methanol (24 mL) was treated with 20 drops of HCl, heated at reflux for 6 hours, and concentrated to provide the desired product (1.07 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06831175B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-98d9bf2f222f4895a899c773c23506c4 |
| Source note | uspto-grants-2004_12 |