HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 85843425, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Tert-Butyl nitrite | HCID 10906 | — |
| Reactant | 5-Bromo-1-indanone | HCID 520695 | — |
| Product | HCID 85843425 | HCID 85843425 | 76% |
Reaction Steps
A solution of 5-bromo-1-indanone (1.8 g, 8.5 mmol) in ethanol (150 ml) was cooled to 0° C., treated with t-butylnitrite (2.1 ml), stirred at room temperature for 2 hours, filtrated and washed the desired product with ether. The yield is 76%. MS (DCI/NH3) m/e 242 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06831175B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-b1c7980cd0bd486aabc9167f6b438dbb |
| Source note | uspto-grants-2004_12 |