HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → (6-Bromo-cinnolin-4-yl)-phenyl-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 6-Bromo-4-chlorocinnoline | HCID 12448078 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | (6-Bromo-cinnolin-4-yl)-phenyl-amine | HCID 22607560 | 62% |
Reaction Steps
A solution of Example 34D (500 mg; 2.5 mmol) and aniline (1.5 mL) in MeOH (11 mL) was stirred at r.t. for 2.5 hrs, the resulting precipitate was collected, rinsed with water and dried under vacuum to provide the desired product (400 mg; 62%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06831175B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-0f9f53e939e048faaae75e14c13c124a |
| Source note | uspto-grants-2004_12 |