HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl vinyl ether → HCID 20745618, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl vinyl ether | HCID 8023 | — |
| Reactant | 2-(Tricyclo(3.3.1.1'3,7)dec-1-yl)ethanol | HCID 110810 | — |
| Catalyst | Mercurous acetate | HCID 61181 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 20745618 | HCID 20745618 | — |
Reaction Steps
36 g (0.2 mol) of 1-admantaneethanol and 72 g (1.0 mol) ethyl vinyl ether were put into a round bottom flask to be dissolved in 100 mL tetrahydrofuran (THF), followed by adding 5 mol % of mercury acetate. Thereafter, the reaction product was reacted for approximately 12 hours under a reflux condition.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06833230B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-4e0b264b1e7c46e7923063593ba48f2f |
| Source note | uspto-grants-2004_12 |