Ethyl vinyl ether → HCID 20745618, compound

HRID 2307837Notes

Reaction equation

HRID 2307837 reaction equation
[C:1]12([CH2:11][CH2:12][OH:13])[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[CH2:2]1)[CH2:8]2.[CH:14](OCC)=[CH2:15]>O1CCCC1.C([O-])(=O)C.[Hg+]>[CH:14]([O:13][CH2:12][CH2:11][C:1]12[CH2:8][CH:7]3[CH2:6][CH:5]([CH2:4][CH:3]([CH2:9]3)[CH2:2]1)[CH2:10]2)=[CH2:15]

Participants

5

Reactant 2

HCID 8023Ethyl vinyl etherHCID 1108102-(Tricyclo(3.3.1.1'3,7)dec-1-yl)ethanol

Product 1

HCID 20745618HCID 20745618, compound

Reagents, catalysts & solvents 2

HCID 61181Mercurous acetateCatalystHCID 8028TetrahydrofuranSolvent

Procedure

36 g (0.2 mol) of 1-admantaneethanol and 72 g (1.0 mol) ethyl vinyl ether were put into a round bottom flask to be dissolved in 100 mL tetrahydrofuran (THF), followed by adding 5 mol % of mercury acetate. Thereafter, the reaction product was reacted for approximately 12 hours under a reflux condition.

Workup

  1. customThereafter, the reaction product was reacted for approximately 12 hours under a reflux condition

Sources & evidence

ORD record
ord-4e0b264b1e7c46e7923063593ba48f2f
Source dataset
uspto-grants-2004_12
Patent number
US06833230B2

Reaction notes

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