HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131724693, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | BAY-41-2272 | HCID 9798973 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 131724693 | HCID 131724693 | — |
Reaction Steps
0.3 g (0.83 mmol) of 3-(4-amino-5-cyclopropylpyrimidin-2-yl)-1-(2-fluorobenzyl)-1H-pyrazolo[3,4-b]pyridine from Example 1 is dissolved in 50 ml of hot acetonitrile, and 0.9 ml of 1 N HCl (0.9 mmol) is added. The precipitated crystals are subsequently filtered off with suction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06833364B1 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-3f199e88a62147fe8d15c94d3329e5d5 |
| Source note | uspto-grants-2004_12 |