2-Phenylethanol → HCID 65019353, compound

HRID 230800Notes

Reaction equation

[C:1]1([CH2:7][CH2:8][OH:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.O[C:11]1[CH:16]=[CH:15][C:14]([C:17]([O:19][CH2:20][CH3:21])=[O:18])=[CH:13][CH:12]=1>>[CH2:8]([O:9][C:11]1[CH:16]=[CH:15][C:14]([C:17]([O:19][CH2:20][CH3:21])=[O:18])=[CH:13][CH:12]=1)[CH2:7][C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

Reactant 2

HCID 60542-Phenylethanol

HCID 8434Ethylparaben

Product 1

HCID 65019353HCID 65019353, compoundYield 100.2%

Procedure

2-Phenylethanol (2.0 g) and ethyl 4-hydroxybenzenecarboxylate (2.7 g) were processed in the same manner as in Production Example 11-2 to obtain the entitled compound (4.4 g).

Sources & evidence

ORD record: ord-2b90a384358b43a291932e08e387b764
Source dataset: uspto-grants-2009_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07566781B2

Reaction notes

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