Boron tribromide → HCID 69896758, compound

HRID 2308002Notes

Reaction equation

HRID 2308002 reaction equation
[CH3:1][O:2][C:3](=[O:27])[C:4]1[C:9]([NH:10][CH:11]([CH2:14][CH3:15])[CH2:12][CH3:13])=[CH:8][C:7]([CH3:16])=[N:6][C:5]=1[O:17][C:18]1[CH:23]=[CH:22][C:21]([Cl:24])=[CH:20][C:19]=1[O:25]C.B(Br)(Br)Br>C(Cl)Cl>[CH3:1][O:2][C:3](=[O:27])[C:4]1[C:9]([NH:10][CH:11]([CH2:12][CH3:13])[CH2:14][CH3:15])=[CH:8][C:7]([CH3:16])=[N:6][C:5]=1[O:17][C:18]1[CH:23]=[CH:22][C:21]([Cl:24])=[CH:20][C:19]=1[OH:25]

Participants

4

Reactant 2

HCID 25134Boron tribromideHCID 69898446HCID 69898446, compound

Product 1

HCID 69896758HCID 69896758, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

The title compound was prepared by reacting 2-(4-chloro-2-methoxy-phenoxy)-4-(1-ethyl-propylamino)-6-methyl-nicotinic acid methyl ester with BBr3 in methylene chloride at rt until all starting material was consumed. Standard work-up procedure gave the title compound.

Workup

  1. customThe title compound was prepared
  2. customat rt
  3. customwas consumed

Sources & evidence

ORD record
ord-19081d4188de4ca79c950726a5b98985
Source dataset
uspto-grants-2004_12
Patent number
US06833378B2

Reaction notes

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