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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2308050Generated: October 31, 2026

p-Fluorotoluene-alpha-thiol → HCID 86593389, compound

https://huagongshe.com/reaction/2308050

Reaction equation

Participants

RoleNameHCIDCharge
Reactantp-Fluorotoluene-alpha-thiolHCID 85171—
ReactantSodiumHCID 5360545—
ReactantBenzene, 1-ethynyl-2,4-diMethoxy-HCID 15184633—
ProductHCID 86593389HCID 86593389—

Reaction Steps

A solution of 2,4-dimethoxyphenylacetylene (0.02 mol), 4-fluorobenzyl mercaptan (0.02 mol) and metallic sodium (0.02 g atom) is subjected to the General Procedure to form (Z)-2,4-dimethoxystyryl-4-fluorobenzylsulfide. The title compound is obtained following oxidation of the sulfide, according to the General Procedure.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06833480B2
Source datasetuspto-grants-2004_12
ORD IDord-c5e58107981f46df813c185c98c4ea99
Source noteuspto-grants-2004_12