HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dichloro-3-ethynylbenzene → (Z)-2,3-dichlorostyryl-2-chloro-4-fluorobenzylsulfide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dichloro-3-ethynylbenzene | HCID 178779 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | (2-chloro-4-fluorophenyl)methanethiol | HCID 22026132 | — |
| Product | (Z)-2,3-dichlorostyryl-2-chloro-4-fluorobenzylsulfide | HCID 86593391 | — |
Reaction Steps
A solution of 2,3-dichlorophenylacetylene (0.02 mol), 2-chloro-4-fluorobenzyl mercaptan (0.02 mol) and metallic sodium (0.02 g atom) is subjected to the General Procedure to form (Z)-2,3-dichlorostyryl-2-chloro-4-fluorobenzylsulfide. The title compound is obtained following oxidation of the sulfide, according to the General Procedure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06833480B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-ce50bb29e50f4b6aa7f30ff89fdfd925 |
| Source note | uspto-grants-2004_12 |