HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Ethynyl-2,4-difluorobenzene → HCID 86593402, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Ethynyl-2,4-difluorobenzene | HCID 5063820 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 20488107 | HCID 20488107 | — |
| Product | HCID 86593402 | HCID 86593402 | — |
Reaction Steps
A solution of 2,4-difluorophenylacetylene (0.02 mol), 2-aminobenzyl mercaptan (0.02 mol) and metallic sodium (0.02 g atom) is subjected to the General Procedure to form (Z)-2,4-difluorostyryl-2-aminobenzylsulfide. The title compound is obtained following oxidation of the sulfide, according to the General Procedure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06833480B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-7bf3e3b8055c4a728950f0be9fcbff75 |
| Source note | uspto-grants-2004_12 |