HCID 9814764, compound → HCID 9878521, compound

Participants

Reaction Conditions

Reaction Steps

0.8 g (2.7 mmol) of 4-(8-nitroquinolin-3-yl)-1,4-diazabicyclo[3.2.2]nonane, in suspension in a mixture of 8 ml of water and 4 ml of acetic acid, is introduced into a 25 ml three-necked round-bottomed flask and the suspension is heated at 40° C.; 0.43 g (7.7 mmol) of iron are then added, in two portions, and the mixture is heated at 50° C. for 1 h.

Provenance & Evidence