HCID 12134605, compound → HCID 12134602, compound

Participants

Reaction Conditions

Reaction Steps

The titled compound of Example 4 (1.22 g, 4.53 mmol) was dissolved in 10 ml of methanol, and added 10% (w/v) Pd/C as a catalyst, followed by stirring for 24 hours at 25° C. Then, the reaction mixture was filtered to give a filtrate, which was then dried under vacuum to obtain a solid compound. The solid compound was recrystallized with ethanol to prepare the titled compound (0.702 g, 65%, m.p. 161-167° C.).

Provenance & Evidence