Methanol → HCID 178493814, compound

Participants

Reaction Steps

The titled compound of Example 5 (0.367 g, 1.53 mmol), triazine (0.19 g, 2.3 mmol) and piperidine (0.015 ml, 0.153 mmol) was dissolved in 10 ml of methanol, followed by refluxing for 4 hours to obtain a white solid, which was then cooled down to a room temperature. The solid compound was filtered, washed with methanol and dried under vacuum to prepare the titled compound (0.240 g, 63%, m.p. 246-251° C.).

Provenance & Evidence