HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dimethylaniline → (3,5-Dimethylphenyl)-(7-methoxymethyl-[1,4]-dioxano[2,3-g]quinazolin-4-yl)-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dimethylaniline | HCID 7949 | — |
| Reactant | 4-Chloro-7-methoxy methyl-[1,4]dioxano[2,3-g]quinazoline | HCID 11161454 | — |
| Product | (3,5-Dimethylphenyl)-(7-methoxymethyl-[1,4]-dioxano[2,3-g]quinazolin-4-yl)-amine | HCID 9903075 | 29% |
Reaction Steps
The titled compound (10 mg, 29%, m.p. 268-270° C.) was prepared in a similar manner as in Example 8, except for employing 4-chloro-7-methoxymethyl-[1,4]dioxano[2,3-g]quinazoline (26 mg, 0.1 mmol) and 3,5-dimethylaniline (24 mg, 0.2 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06835735B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-c7ba345953d6445fb53de57599af5e95 |
| Source note | uspto-grants-2004_12 |