HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2-chlorophenol → 4-Bromo-2-chloroanisole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2-chlorophenol | HCID 19859 | — |
| Reactant | 5-Methoxy-2-nitrobenzotrifluoride | HCID 548517 | — |
| Product | 4-Bromo-2-chloroanisole | HCID 3016537 | 93% |
Reaction Steps
Starting from 4-bromo-2-chlorophenol (22 g, 110 mmol) in place of 4-nitro-3-trifluoromethylphenol, the title compound (22 g, 93%, m.p. 69-71° C.) was synthesized in essentially the same manner as described above for 4-nitro-3-trifluoromethylanisole in Step 1, Scheme 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06835745B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-2b12c03f1179406982bde15ca5b5ca76 |
| Source note | uspto-grants-2004_12 |