HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylene → HCID 22601781, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylene | HCID 6325 | — |
| Reactant | Methyl 2-(3-bromophenyl)acetate | HCID 11746402 | — |
| Product | HCID 22601781 | HCID 22601781 | — |
Reaction Steps
Methyl 3-bromophenylacetate (8.0 g, 34.9 mmol) was reacted with ethylene using the procedure described in Example 6, step 1. The crude reaction product was purified by column chromatography (SiO2, 5% EtOAc in petroleum ether) to give 3,3′-bis-[(carbo-methoxy)methyl]stilbene and methyl 3-(ethenyl)phenyl-acetate as a white solid mixture.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06835753B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-cd3e82fb4f8049398d6dcdaec2576658 |
| Source note | uspto-grants-2004_12 |